Pre-lab
exercise for the week of 9/11/2000
This exercise is due two hours before
your lab session
1.
Use
a pen(cil) and paper to draw a Lewis structure of (BH4)-1
before answering the following questions.
What is the shape of this anion
(focus on the boron)? What is
the formal charge of each atom in the molecule? How are its bonds polarized?
2.
Your
lab procedure calls for you to monitor your reduction reaction using TLC. Provide a description of how you intend to
accomplish this.
3.
At
the end of the lab, we will analyze the product composition by GC-MS (a mass
spectroscopy technique). Based on the
minimal introduction to mass spectroscopy you've received, how might you tell
the starting ketone from the product alcohol?